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Mohammad Ali Bodaghifard

Mohammad Ali Bodaghifard

Academic rank: Associate Professor
ORCID: https://orcid.org/0000-0001-9732-4746
Education: PhD.
ScopusId: 6507703429
HIndex:
Faculty: Science
Address: Arak University
Phone:

Research

Title
Palladium-melamine complex anchored on magnetic nanoparticles: A novel promoter for C-C cross coupling reaction
Type
JournalPaper
Keywords
Palladium Nanocatalyst Magnetic separation Heck reaction Magnetic nanoparticles
Year
2019
Journal J ORGANOMET CHEM
DOI
Researchers Mohammad Ali Bodaghifard

Abstract

A palladium-melamine complex deposited on Fe3O4@SiO2 nanoparticles (MNPs-Mel-Pd) was considered as an effective catalyst for C-C cross-coupling (Mirozoki-Heck) reaction. Surface and magnetic properties of the prepared core-shell hybrid nanocatalyst was characterized using Fourier transform infrared spectroscopy, X-ray diffraction, thermogravimetric analysis, energy-dispersive X-ray, vibrating sample magnetometry, transmission and scanning electron microscopy techniques and ICP/OES analysis. It was found that the heterogeneous nanocatalyst could be recovered simply and reused numerous times without loss of its catalytic activity. The advantages of this new methodology are: isolation of highly pure products without chromatography techniques, reusability of the catalyst using a magnet, easy workup procedure and negligible leaching of palladium.