2024 : 4 : 14
Mohammad Ali Bodaghifard

Mohammad Ali Bodaghifard

Academic rank: Associate Professor
ORCID: https://orcid.org/0000-0001-9732-4746
Education: PhD.
ScopusId: 6507703429
Faculty: Science
Address: Arak University
Phone:

Research

Title
Mechanistic study on a novel pseudo-five-component synthesis of 4 H-thiopyrans
Type
JournalPaper
Keywords
carbon disulfide, isothiocyanate,mechanistic study,multicomponent reaction, thiopyrans
Year
2017
Journal Phosphorus, Sulfur, and Silicon and the Related Elements
DOI
Researchers Sajad Asadbegi ، Akbar Mobinikhaledi ، Mohammad Ali Bodaghifard

Abstract

The use of carbon disulfide provides a novel and efficient route for the synthesis of thiopyrans. Herein we describe a study on the pseudo-five-component preparation of 4 H- thiopyran derivatives by condensation of aldehydes, malononitrile, carbon disulfide, and primary amines in the presence of triethylamine. Separation and identification of the reaction intermediates and products, additional starting materials designing, repeating of the reaction, and determining of the products, NMR, and GC-mass analysis of the reaction mixtures, were used to evaluate and confirm the reaction pathway.