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Gholamreza Nabiyouni

Gholamreza Nabiyouni

Academic rank: Professor
ORCID: https://orcid.org/0000-0001-8703-9693
Education: PhD.
ScopusId: 6602215199
HIndex:
Faculty: Science
Address: Arak University
Phone:

Research

Title
A Simple Method for Synthesis of PbS Nanoparticles Using 2-Mercaptoethanol as the Capping Agent
Type
JournalPaper
Keywords
Nanoparticles, capping agent, lead sulfide
Year
2012
Journal High Temperature Materials and Processes
DOI
Researchers Gholamreza Nabiyouni ، Parviz Boroojerdian ، Kambiz Hedayati ، Davoud Ghanbari

Abstract

Lead sulfide nanoparticles were synthesized at room temperature via a simple chemical reaction. In this synthesis, 2-mercaptoethanolwas used as the capping agent and sodium sulfide was used as a sulfur source. The products were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), ultraviolet-visible (UV-vis) spectroscopy and Fourier transform infrared (FT-IR) spectroscopy Electron microscopy study showed that without using a capping agent the bulk PbS is obtained, while adding the mercaptoethanol leads to production of nanoparticles. We found that the electronic absorption spectra as well as the particle sizes depend on the used capping agents. Two exitonic peaks with a large blue shift were observed when mercaptoethanol was used.