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Akbar Mobinikhaledi

Akbar Mobinikhaledi

Academic rank: Professor
ORCID: https://orcid.org/0000-0002-9732-7282
Education: PhD.
ScopusId: 6701730547
HIndex:
Faculty: Science
Address: Arak University
Phone:

Research

Title
Preparation of Core/Shell CaO@SiO2-SO3H as a Novel and Recyclable Nanocatalyst for One-Pot Synthesize of Dihydropyrano[2,3-c] Pyrazoles and Tetrahydrobenzo[b]Pyrans
Type
JournalPaper
Keywords
Green chemistry . Eggshell . Sulfonic acid . Core/shell .Dihydropyrano[2, 3-c]pyrazoles . Tetrahydrobenzo[b]pyrans
Year
2021
Journal SILICON-NETH
DOI
Researchers Fatemeh Sameri ، Akbar Mobinikhaledi ، Mohammad Ali Bodaghifard

Abstract

The core/shell CaO@SiO2-SO3H nanoparticles were prepared by stabilizing of sulfonic acid on the surface of silica-coated CaO nanoparticles. The structure of CaO@SiO2-SO3H was characterized by Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM), energy dispersive X-ray spectroscopy (EDS), wavelength-dispersive X-ray spectroscopy (WDX) and thermal gravimetric analysis (TGA). CaO@SiO2-SO3H was used as a new acidic catalyst for green synthesis of dihydropyrano[2,3-c]pyrazoles and tetrahydrobenzo[b]pyrans via one-pot three-component reactions with good to excellent yields. This catalyst could be recycled and reused for six runs without significant loose of activity.