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Akbar Mobinikhaledi

Akbar Mobinikhaledi

Academic rank: Professor
ORCID: https://orcid.org/0000-0002-9732-7282
Education: PhD.
ScopusId: 6701730547
Faculty: Science
Address: Arak University
Phone:

Research

Title
Sulfanilic acid-functionalized silica-coated magnetite nanoparticles as an efficient, reusable and magnetically separable catalyst for the solvent-free synthesis of 1-amido- and 1-aminoalkyl-2-naphthols
Type
JournalPaper
Keywords
-
Year
2014
Journal RSC ADVANCES
DOI
Researchers Hassan Moghanian ، Akbar Mobinikhaledi ، AG Blackman ، E Sarough Farahani

Abstract

Sulfanilic acid-functionalized silica-coated nano-Fe3O4particles (MNPs–PhSO3H) have been prepared as a reusable heterogeneous acid catalyst using a facile process. The catalytic performance of this novel material has been studied in the synthesis of 1-amido- and 1-aminoalkyl-2-naphthol derivativesviaa one-pot three-component condensation reaction of aldehydes, 2-naphthol, and amides/urea/amines in good to excellent yields, under solvent-free classical heating conditions. The catalyst was easily separated from the reaction mixture with the assistance of an external magnetic field and reused for several consecutive runs without significant loss of its catalytic efficiency. Results obtained from transmission electron microscopy (TEM), scanning electron microscope (SEM), powder X-ray diffraction (XRD) and sample magnetometery (VSM) show that the synthesized magnetic nanocomposites are superparamagnetic with a size range of 15–30 nm